Application of gas chromatography in the detection of VOC content in paint
2014.09.24 10:50With the development of technology to improve people's living standards and enhance the rapid development of the coatings industry and environmental awareness , in addition to the requirements of the decorative material attractive and durable , but also required to comply with the requirements of environmental protection and health benefits .
Gas chromatography is a technique may be qualitative , quantitative separation and analysis techniques. Because of its high separation efficiency , rapid analysis , good selectivity。 Gas chromatography is widely used in the field of contaminant analysis in environmental samples , quality control and other industrial products .
Under the new provisions of the national standard GB18582-2008 , and must be measured for paint products such as water and water-based wall paint wall putty using gas chromatography , detection of which the sum of the content of volatile organic compounds VOC and benzene , toluene , xylene .
GC is a large precision instruments in the paint analysis, one of the most widely used instrument .
Principle
After the sample is diluted by gas chromatography analysis for all the samples in the separation of volatile organic compounds , the qualitative identification of the test compound , using the internal standard method to test its content.
Equipment
Gas chromatograph includes the following configuration
1 shunt device inlet, and vaporization chamber liner can be replaced
2 temperature-programmed controller
3 detector , a flame ionization detector
4 column polydimethylsiloxane capillary column
5 injector, a microsyringe , 10 l
6 vials with about 20 ml glass bottle with a tight lid .
7 balance, accuracy of 0.1 mg
Because of its unique properties in coatings, Gas chromatographic analysis methods has been quite popular , as early as 1997 have used this method to detect the Nippon Paint , Watson 's numerous chemical plants and other products, residual monomers , free monomer , solvents and VOC analysis and other aspects of the application has been successful for the coatings industry development and environmental protection technology provides a good guarantee . standardization in the field of paint analysis , gas chromatography analysis by showing , automation and specialization trend has been formed to develop and commercialize applications that meet specific criteria and application -specific software analysis system has become in recent years, major technology progress flag.